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Development and validation of a LC method for the separation and determination of the anticancer-active FeIII(4-methoxy-salophene) using the new second-generation monolith

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Al-Azhar University – Gaza
El Deeb S.; Ma B.N.; Gust R.
El Deeb, Sami (14059838300); Ma, Benjamin N. (55882160800); Gust, Ronald (7005963725)
14059838300; 55882160800; 7005963725
2012
Journal of Separation Science
Development and validation of a LC method for the separation and determination of the anticancer-active FeIII(4-methoxy-salophene) using the new second-generation monolith
35
24
3434
3438
Institute of Pharmacy, Freie Universität Berlin, Berlin, Germany; Department of Pharmaceutical Chemistry, Al-Azhar University-Gaza, Palestinian Territories, Gaza, Israel; Department of Pharmaceutical Chemistry, Institute of Pharmacy, University of Innsbruck, A-6020 Innsbruck, Innrain 80-82, Austria
El Deeb S., Institute of Pharmacy, Freie Universität Berlin, Berlin, Germany, Department of Pharmaceutical Chemistry, Al-Azhar University-Gaza, Palestinian Territories, Gaza, Israel; Ma B.N., Department of Pharmaceutical Chemistry, Institute of Pharmacy, University of Innsbruck, A-6020 Innsbruck, Innrain 80-82, Austria; Gust R., Department of Pharmaceutical Chemistry, Institute of Pharmacy, University of Innsbruck, A-6020 Innsbruck, Innrain 80-82, Austria
R. Gust; Department of Pharmaceutical Chemistry, Institute of Pharmacy, University of Innsbruck, A-6020 Innsbruck, Innrain 80-82, Austria; email: ronald.gust@uibk.ac.at
8
10.1002/jssc.201200734
Anticancer; Fe<sup>III</sup>(4-OMe-salophene); Monolithic silica columns
Antineoplastic Agents; Chromatography, Liquid; Ferric Compounds; Limit of Detection; Reproducibility of Results; Atomic absorption spectrometry; Body fluids; Iron; Methanol; Separation; Silica; Spectroscopic analysis; antineoplastic agent; ferric(4 methoxy salophene); unclassified drug; Anticancer; Atomic absorption spectroscopy methods; Calibration curves; High resolution; In-vitro; Iron atoms; Mobile phase; Monolithic columns; Monolithic silica; Monolithic silica columns; Phosphate buffers; Quantitation limits; Serum albumin; Working range; article; concentration (parameters); drug determination; drug isolation; flow rate; in vitro study; limit of detection; limit of quantitation; liquid chromatography; pH; priority journal; Iron compounds