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Repeatability of monolithic HPLC columns while using a flow program

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Al-Azhar University – Gaza
Kaminski L.; El Deeb S.; Wätzig H.
Kaminski, Lukas (24447927000); El Deeb, Sami (14059838300); Wätzig, Hermann (55963552800)
24447927000; 14059838300; 55963552800
2008
Journal of Separation Science
Repeatability of monolithic HPLC columns while using a flow program
31
10
1745
1749
Institute of Pharmaceutical Chemistry, Technical University Braunschweig, D-38106 Braunschweig, Beethovenstrasse 55, Germany; Department of Pharmaceutical Chemistry, Al-Azhar University -Gaza, Gaza, Palestinian Territory, Egypt
Kaminski L., Institute of Pharmaceutical Chemistry, Technical University Braunschweig, D-38106 Braunschweig, Beethovenstrasse 55, Germany; El Deeb S., Department of Pharmaceutical Chemistry, Al-Azhar University -Gaza, Gaza, Palestinian Territory, Egypt; Wätzig H., Institute of Pharmaceutical Chemistry, Technical University Braunschweig, D-38106 Braunschweig, Beethovenstrasse 55, Germany
H. Wätzig; Institute of Pharmaceutical Chemistry, Technical University Braunschweig, D-38106 Braunschweig, Beethovenstrasse 55, Germany; email: h.waetzig@tu-bs.de
20
10.1002/jssc.200700681
Fast HPLC; Flow programming; Monolithic columns; Repeatability
Area Under Curve; Chemistry, Pharmaceutical; Chromatography; Chromatography, High Pressure Liquid; Drug Stability; Glyburide; Hypoglycemic Agents; Models, Chemical; Reference Standards; Reproducibility of Results; Solvents; Sulfonylurea Compounds; Technology, Pharmaceutical; Time Factors; Chemotherapy; Columns (structural); Degradation; Drug delivery; Drug dosage; Semiconductor switches; Separation; Shearing machines; Sugar (sucrose); Sulfate minerals; glibenclamide; glimepiride; oral antidiabetic agent; solvent; accuracy; area under the curve; article; controlled study; drug degradation; drug determination; drug structure; flow rate; high performance liquid chromatography; intermethod comparison; priority journal; qualitative analysis; reproducibility; separation technique; Anti-diabetic drugs; Applied (CO); Degradation products; Glibenclamide; Glimepiride; high flow; High performance liquid chromatographic (HPLC) methods; High performance liquid chromatography (HPLC) columns; Peak areas; Retention times; Run time; Flow rate